Full Text Searchable PDF User Manual
1
Vacuum Drying
Purging
Oven
(Controlled by Microchips with Timing Function)
Operation Manual
Our Lawyers Say:
This is a general-purpose vacuum oven for professional, industrial or educational use.
It is suitable for a working environment where no
flammable, volatile or combustible materials are being heated.
This oven is not intended for hazardous use.
Your satisfaction and safety require a complete understanding of this unit.
Read the instructions thoroughly and be sure all operators are given
adequate training before attempting to put the unit in
service.
This equipment must be used only for its intended application.
Our Design Engineers Say:
Your oven is intended for use indoors, at temperatures between 25°C and 40°C,<
80% Relative Humidity.
Extreme external
temperatures or humidity levels can affect the oven’s ability
to control temperature.
* If sample releases vapor under heating, place a dryer between the vacuum pump and the oven to
avoid vapor damage to the pump.
* Always wear thermal
gloves and protective goggles during operation.
* Always use the power cord that comes with the unit. Never modify the cable.
* Keep oven away from any electromagnetic interference. Do not unplug the oven during normal
operation.
*Do not try to heat flammable/explosive materials or materials that may release corrosive substances.
*When vacuuming is done, the vacuum valve should be closed first before turning off the power to
the vacuum pump; otherwise vacuum pump oil may backflow into the oven.
*Keep the oven clean at all time; clean the glass and chamber with soft cotton cloth after each use.
*If oven is to be kept idle for a long time, protect its circuit board with neutral grease or Vaseline to
avoid corrosion, and cover the oven entirely to keep it away
from dust and moisture.
2
2. Features and specifications
These ovens can greatly reduce drying time by maintaining a consistent vacuum level within the chamber. Oven operation is
controlled by a digital microcontroller which is used to achieve
temperature precision and accuracy. our vacuum ovens goes
through a 24-hour vacuum leak test before leaving our factory.
*Dual layer observation window with solid tempered safety glass.
*Radiant wall heating system(Surfacce Heating Tech) provides optimal
uniformity and conserves chamber space.
*Easy-to-clean 304 stainless steel interior for exceptional durability and ease of maintenance.
*Adjustable-force latch and door sealing gasket maintain consistent vacuum level.
Model:DZF-6050 Vacuum Oven/1.9CF
220V 50/60Hz 1-PH
5.9
Amps
USA standard 3-prong plug
1,
3
00 watts.Mica Heating Pads JP tech
Stainless steel SUS304#
Power
Power connection
Heaters
Chamber Material
Temperature controller
Low proportional gain, PID control for heater output
by microcomputer
Ambient to 100°C
Celsius
/Fahrenheit
±1
°C
/ ±1
°
F
1-9999 minutes
415 x 370 x 345mm (WxDxH)
Come with 4 removable aluminum heating shelves.
710 x 550x 550mm(WxDxH)
840 x 680 x 680mm(WxDxH)
Better than 500 microns/millitorrs depend on the Vacuum Pump.
<133Pa
KF-25 Vacuum Port
&
1/2
”
-10mm Hose Port (Gas
Back Fill System)
Silicone
Built-in circuit breaker, overheat protector
Temperature range
Temperature units
Temperature accuracy
Dwelling timer range
Chamber dim
Shelf
Unit dimensions
Shipping dimensions
Vacuum level
Maximum Vacuum
Vacuum Outlet/Gas Inlet
Door gasket material
Safety
Tempered Glass
Shipping weight
15mm tempered safety glass
8
1
kgs(Packed into Export Woodencase).
3
Power
Power connection
Heaters
Chamber material
Temperature controller
Temperature range
Temperature units
Temperature accuracy
Dwelling timer range
Chamber dim
Shelf
Model:DZF-6090 Vacuum Oven/3.2
CF
220V 50/60Hz 1-PH
4.5Amps
USA standard 3-prong plug
1,000 watts.Built inside
2
aluminum shelves for the
fastest, most energy efficient and most even heating.
SUS304#
Low proportional gain, PID control for heater output
by
microcomputer
Ambient to
10
0°C
Celsius
/Fahrenheit
±1
°C
/ ±1
°
F
1-9999 minutes
18 x 18 x 18" (WxDxH) divided into three sections, arranged vertically.
2 non-removable
aluminum heated shelves,divided into two 17.5 x 17.5 x4" (WxDxH) sections,
arranged vertically.
30.9 x 23.4x 27.5"(WxDxH)
33.9 x 27.4 x32.5"(WxDxH)
Better than 500 microns/millitorrs depend on the
Vacuum Pump.
<133Pa
KF-25 Vacuum Port
&
1/2
”
-10mm Hose Port (Gas Back Fill System)
Silicone
Built-in circuit breaker, overheat protector
1
9
mm tempered safety glass
1
1
0KG
Unit dimensions
Shipping dimensions
Vacuum level
Maximum Vacuum
Vacuum Outlet/Gas Inlet
Door gasket material
Safety
Tempered Galss
Shipping weight
Custom Extra 2 removal aluminum shelves for 3.2
CF
Vacuum Oven.
4
Power
Power connection
Heaters
Chamber material
Temperature controller
Temperature range
Temperature units
Temperature accuracy
Dwelling timer range
Chamber dim
Shelf
Model:DZF-6090 Vacuum Oven/3.4
CF
220V 50/60Hz 1-PH
6.8
Amps
USA standard 3-prong plug
1,
5
00 watts.Built inside
3
aluminum shelves for the
fastest, most energy efficient and most even heating.
S
US#304
Low proportional gain, PID control for heater output
by microcomputer
Ambient to
10
0°C
Celsius
/Fahrenheit
±1
°C
/ ±1
°
F
1-9999 minutes
18 x 18 x 18" (WxDxH) divided into three sections, arranged vertically.
3 non-removable aluminum heated shelves,divided into two 17.5 x 17.5 x5" (WxDxH) sections,
arranged
vertically.
30.9 x 23.4x 27.5"(WxDxH)
33.9 x 27.4 x32.5"(WxDxH)
Better than 500 microns/millitorrs depend on the Vacuum Pump.
<133Pa
KF-25 Vacuum Port
&
1/2
”
-10mm Hose Port (Gas Back Fill System)
Silicone
Built-in circuit breaker, overheat protector
19mm tempered safety glass
1
2
0KG
Unit dimensions
Shipping dimensions
Vacuum level
Maximum Vacuum
Vacuum Outlet/Gas Inlet
Door gasket material
Safety
Tempered Glass
Shipping weight
Custom Extra 3 removal aluminum shelves for 3.
4CF
Vacuum Oven.
5
Power
Power connection
Heaters
Chamber material
Temperature controller
Model:DZF-6210 Vacuum Oven/7.8
Plus
220V 50/60Hz single phase
9.09
A
USA standard 3-prong plug
2000watts. Built inside
5
aluminum shelves for the
fastest, most energy efficient and most even heating.
SUS 304#
Low proportional gain, PID control for heater output
by microcomputer
Ambient to
10
0°C
Celsius
/Fahrenheit
Temperature range
Temperature units
Temperature accuracy
Dwelling timer range
Chamber dim
Shelf
±1
°C
/ ±1
°
F
1-9999 minutes
22 x 24 x 25" (WxDxH) divided into three 22 x 24 x
5
"
(WxDxH) sections, which arranged vertically.
5
non-removable aluminum heating shelves with individual in-oven temp sensor, heater and
controller (additional stackable shelves
available)
35 x 31 x 38" (WxDxH)
38 x 35 x 43" (WxDxH)
Better than 500 microns/millitorrs depend on Vacuum Pump.
<133Pa
13.5 CFM single stage
KF-25 Vacuum Port
&
1/2
”
-10mm Hose Port (Gas Back Fill System)
Silicone
19mm
Unit dimensions
Shipping dimensions
Vacuum level
Maximum
vacuum pressure
Vacuum Pump
Vacuum Outlet/Gas Inlet
Door gasket material
Tempered Glass
Unit/shipping weight
220Kgs
Custom Extra
5
removal aluminum shelves for
7.8Plus
Vacuum Oven.
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3. Guidelines
using the vacuum oven
1. Put your
target
into the
vacuum
oven;
C
lose the door;
C
lose the
black
vacuum release; open the vacuum valve
and turn on the power to the vacuum pump to start the purging process
,
When vacuum level in the oven reaches
30 inch mercury
(or read
76cmHg);
C
lose the vacuum valve first
BEFORE
turn off the vacuum pump.
2. Turn on the
Vacuum
oven,
S
et target temperature and confirm it. Temperature in the oven starts to rise and
the heating indicator will blink.
3. If your target temperature is low, setting can be done twice to minimize temperature spike. For example, if
target temperature is 40°C, the first target temperature value can be set to 30°C, and when temperature rises
excessively and starts to drop, set the temperature one more time to 40°C.Thus,temperature overshooting can be
reduced or prevented and temperature dwelling state can be started ASAP.
4. Length of drying time should be selected based on humidity level of your sample. In case drying time is long
and vacuum level reduces, it is
necessary to purge the oven again to restore desired vacuum level (make sure
your vacuum pump can work at your target temperature).
5.
A
fter
purging
drying process done, turn off the oven; open the vacuum release valve before opening the door.
It is possible that the sealing gasket may stuck onto the glass door and the door cannot be open easily. Wait a
while until the gasket restores itself before trying to open the door again.
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4.
Preset target temperature “SP” & Purging working time St
Running
mode: after the oven is first turned on, controller will be in running mode.
Setting mode: hold and “Set” button for
6 seconds in running mode to enter into the setting mode.
Controller will return to running mode automatically if no action is taken in 60
seconds.
4-1. Setting target temperature and dwelling time
1. Plug in power cable, switch on circuit breaker in the back and turn on the oven.
2
. Press ‘Set’ button once, controller will display “SP”, now use “Shift”, “Decrease” or “Increase”
button to set
your target
temperature.
3
. Press ‘Set’ again to confirm, controller will display “S
t
”, now use “Shift”, “Decrease” or “Increase” button to set dwelling time
in minutes (you can set it to display in hours with the “Hn”
setting). Oven starts timing the
first time actual temperature re
aches target temperature. If “S
t
” is
set to zero, oven will
continue to run at target temperature until turned off manually.
4
. Press ‘Set’ again to confirm all settings.
5. When dwelling time is up, the controller will
disp
lay “End” and buzz for 60 seconds. It can be
muted by pressing any button.
6
. Press and hold “Reset” for 3 seconds to restart oven operation.
7. During heating, if alarm is set and actual temperature is over that limit, buzzer will sound continuously a
nd “ALM” light will
come on. Press any key to mute it.
Prompts
Names
Description
Sp
St
Target Temperature value
Dwelling time
range Default
value
Amb+10
℃～
100
℃
0-9999 (0) minutes
Single point control set temperature(
℃
)
0 = continuous heating, use co
de “Hn” to
change unit
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*
MENU I & MENU II
Under running mode, press and hold “Set” button for
6
seconds;
C
ontroller will display “Lc”.
Enter
3
and press
“Set” for the menu in
MENU I
E
nter
9
and press “Set” for menu in
MENU II
.
After you done with the setting
change, press and hold “Set” for 3 seconds to
save and exit to running mode
.
MENU I:
Prompt
Name
Description
When Lc = 3, controller enters into the menu below
If SV>(SP+AL), ALM light comes up, buzzer sounds and oven stops
heating
Represents the specific control method of the relay.
Pass Key
Over-temp alarm
Control Cycle
Lc
AL
T
P
Proportional
Increase P reduce temperature overshooting,decrease P to allow faster heating rate.
default Value
3
0~100(5)
5
35
I
Integral
Increase I to lower temperature
fluctuation
Adjusted to reduce temperature overshooting.
1~1000s
(200s)
D
Differential
0~1000s
(200s)
Pb
-10~10
(0)
Ambient
adjustment
PK
Et
Hot adjustment
Timing Function
-999~999
(0)
0~2(2)
Offset the temperature difference ambient and oven when it is turn off.
Pb = temperature measured by exterior thermocouple(s)
–
temperature displayed by
controller
Offset the temperature difference between the controller and actual reading inside
the oven. (use the calibration formula in 5-2 section)
0: no timer function
1: with timer function, SV window will always display dwelling time.
2: with timer function, SV window will display dwelling time after oven temperature
reaches target temperature.
9
MENU II:
Prompt
Name
Description
default Value
Lc
Pass key
Shut off
When Lc = 9, controller enters into the menu below
9
Co
If SV>(SP+Co), ALM light comes up, buzzer sounds and oven stops heating
0~50(5)
Heat Function
Timer unit
Hn
En
0: minute 1: hour
0-1 (0)
0~1(0)
Timer end mode
0: stop temperature controller when dwelling time is over
1: continue to display temperature when dwelling time is over
Lt
Max Watt Output Max Watt heating Output
0~100
(
100
)
0~1
oP
Door Controll
Function
0,Door Controller Function(Close)
1,Door Controller Function (Open)
*The Function is under innovation.
(1)
rH
Max temperature Set maximum temperature the controller can go to
(Do NOT modify. Setting max temperature too high could permanently damage your oven)
0~400
(100)
10
AutoTune
1:)
Plug on
220Volts 50/60Hz Open
the power switch
.
2:)Press "set" then increase or decrease to target temp (eg
.
Sp=
33
).
then press "set" (St=0) and then press "set"
6 seconds
save and exit.
It is easily to operate in default leaving factory for
purging drying process
.
If client are not
satisfied with target temp (always find over heat problem)during heat process.
How to make it normal working? Easily Follow below steps:
1:)Power Off Vac Oven and Open Door Cool down inside oven temp below 33deg C----(Cool Down 30-50minutes).
2:)
Power On
.Then Press "set" 6" it will showing Lc" increase 3 then entry into "Menu I" Press "Set" again to find out "P"
increase "35" press "set" again I" increase "200" press "set" then D" increase "200" then press "set" 6" save and exit.
3:)Press "AT" 6" it will entry into Autotune Process for (eg
33
deg C ) The "AT" light flashing and working to find out the best
PID data and save and exit
(once it finished the light always light on).Then Power Off. Wait 30 minutes.
Autotune Process
function:in order to avoid Over Heating Temp(eg. You want 48deg C if AT,it will not over heat higher than
<50deg C) to protect material.
Caution:Autotune Process 50deg C ( 30-50deg C ) the uniform temp working well and without over heat temp.
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5. How to Calibrate your vacuum oven.
NOTE: Before calibrating your oven, make sure you are familiar with basic oven heating operation.
Every oven has been calibrated and tested before leaving our factory, usually self calibration is not necessary.
However, if the temperature requirements are very strict, or if target temperature is set around upper or lower
limits of the oven temperature range, the measured temperature might not be accurate against the actual
temperature in the oven.
5-1. Calibration by Auto-Tune (AT)
Use auto-tune to set a more accurate temperature control and faster heating rate.
a. Set temperature to your maximum target temperature, press “Set” to confirm.
b. Under running m
ode, press and hold “Shift/AT” button for 5 seconds until the indicating light “Run/AT”
starts to blink. The oven is now in PID auto-tune mode.
c. After two cycles of fluctuation, auto-tune is done and the AT light goes off. This could take a few hours. The
“Set” button is disabled during this period.
d. New PID parameters are automatically saved for future use.
e. Now set the target temperature. You will be ready to use the oven.
5-2. Calibration by formula
First, calculate the offset value using the formu
lation below. Then press and hold “Set” button for 3
seconds;
controller will display “Lc”. Enter 3 and press “Set”. Go to “PK” and set it to your calculated offset value.
Press and hold “SET” for 3 seconds to confirm.
Offset value = (temperature measured by exterior thermocouple(s)
–
temperature displayed by
controller) x 1000 / temperature displayed by controller
5-3. Calibration by adjusting PID manually (requires experience and practice)
After an auto-turn, if you still feel that temperature is unstable, you can manually adjust PID. PID adjustment
is a very useful for you to control the oven temperature in an acceptable range but requires some practice and
patience.
After an auto-tune, if you still feel that temperature is unstable, you can manually adjust PID. PID adjustment
is a very useful tool for controlling the oven temperature within an acceptable range, but requires some
practice and patience.
a. First, adjust P whenever you start a PID adjustment. P represents proportion adjustment; increasing P
reduces temperature overshooting, while decreasing P to allow for a faster heating rate. (You may need to try
this step a few times before you get the best result).
b. “I” represents integral time. Increase I to lower temperature fluctuation. It can be use
d to eliminate the
steady-state error after the system enters a steady state by correctly setting P. In other words, I is often used
after P. Give I a big value before decreasing P a little, in order to get to a steady state, and then decrease I to
eliminate errors under the steady state. Check if the PV is in your desired range. Continue to try to change
P and I to get the best result.
c. “D” represents differential time, which can overcome the unstable and oscillating state. Adjust D to reduce
temperature overshooting. It is usually set after I adjustment. Firstly, set D to 0, then gradually increase it to
check if you have an acceptable result (In this process, P and I may also be changed).
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6. Troubleshooting.
Without Power
Without power supply
Broken power cord or Loose plug
Circuit breaker is off
Check power supply
Change power cord
Turn on circuit breaker
PV window is
displaying
Faulty pt100 thermocouple or loose
connection
Check connection or change
thermocouple
“
-----
”, “LLL.L” or “HHH.H”
Faulty temperature controller
If the thermocouple is OK and connection
is good, replace the temperature
controller.
Failure to heat unit
Setting times out
Modify the set time and restart the oven
Check and make sure all connection
Loose connection on temp controller
Faulty controller
Faulty heating element
Replace temperature controller
Replace heating elements
Reset all parameters to default
Check all connections
Parameter error
Temperature control Fail
Loose connection on pt-100 thermocouple
Faulty controller
Replace temperature controller
Adjust preset temperature
Preset temperature too low
Abnormal alarming
Faulty controller
Without Vacuum
Parameter error
Replace temperature controller
Vacuum the oven
for oven temperature
Large temperature
Reset all parameters to default
difference between
Sensor of thermometer has been placed at
incorrect place
Place the sensor on the oven self
PV value and actual
value
13
8. Support
We offer 2 year limited replacement warranty for all electronic parts from the date we shipped goods.
If you find any defective parts caused by manufacturer please feel free to contact us and
we will replace them for you.
420PMU
K
is not responsible for any damage or consequence damage caused by misuse.
After the
warranty period, we will continue to provide support
and spare parts at a reasonable cost.