Buchi B-740 Operation Manual - User Manual

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Operation Manual

096691

�

740

Recirculating Chiller

BÜCHI

Recirculating Chiller

B-740

Contents

B-740 Instructions

96691

Scope of delivery

Safety

Function

Putting into operation

Operation

Maintenance

Taking out of operation

Appendix

en, Version D

(14 pages)

Order no.

Read through these operating instructions
thoroughly before you use the

BÜCHI

Recirculating Chiller

B-740

. Keep these

instructions in the immediate area of the
apparatus so that they can be referred to
at any time.

Chapter 2 contains important safety tips.
Knowledge of these is indispensable for the
safe operation of the apparatus.

Subject to technical alterations without prior notice. No part
of these operating instructions may be reproduced in any
form whatsoever or processed, reproduced or disseminated
using electronic or optical systems without the written per-
mission of Büchi Labortechnik AG. All rights reserved.
Copyright © Büchi Labortechnik AG, 1997

BÜCHI

Recirculating Chiller

B-740

Figure 1: Total view B-740

1 Scope of delivery

Description

Apparatus versions:

Order no.

Büchi Recirculating Chiller B-740 230 V
Model 800 Watt

37740

Model 1400 Watt

37741

Model 2500 Watt

40300

Table 1: Scope of delivery

Enclosed parts:

1 Instructions:
Deutsch

96690

English

96691

French

96692

Italian

96693

Spanish

96694

1 Mains cable PNE, 2,5 m
Type CH

10010

Type Schuko

10016

Type GB

17835

Type AUS

17836

Type USA

10020

1 Packaging cpl.

Table 2: Enclosed parts

1 Scope of delivery

Figure 2: B-740, 2500W

Optional accessories:

Distribution head with taps

37742

Table 3: Optinal accessories

BÜCHI

Recirculating Chiller

B-740

2 Safety

The apparatus is constructed in accordance with state-
of-the art technology and recognized technical safety
regulations.
Nevertheless risks and danger can arise from the appara-
tus:
• if the apparatus is not used according to instructions.
• if the apparatus is operated by insufficiently trained
personnel.

2.1 Symbols

Stop

Information on the dangers which can lead to great damage
to property or to severe or life-threatening injuries.

Warning

Information on the dangers which can lead to damage to
one’s health or to damage to property.

Please note

Information which indicates technical requirements. Non-
compliance can lead to disturbance, uneconomical ope-
ration or production losses.

2.2 Demands on the operator

The apparatus may only be used by persons who have an
overview of the dangers which can develop when operating
the apparatus.

2.3 Regulation use

The Recirculating Chiller is conceived and built as a piece
of laboratory equipment. Its regulation use is the cooling
of closed cycles (e.g. rotary evaporators, reaction vessels
...).

The regulation use of the Recirculating Chiller also includes
its care.

BÜCHI

Recirculating Chiller

B-740

2 Safety

2.4 Nonregulation use

Any and every use other than the above-mentioned as well
as any and every application which does not correspond
to the technical data is a misapplication. The operator
bears the sole risk for any possible damage traced back
to such a use.
In particular, the following uses are improper:

Use of the apparatus in rooms which require explosion-
proof apparatus.

2.5 Safety measures

The wearing of personal protective equipment such as

safety glasses

is necessary.

These operating instructions must, as a component of the
Recirculating Chiller B-740 be available at all times to the
operating personnel at the place of use of the apparatus.
The operator is responsible for the instruction of his or her
personnel. For this purpose these operating instructions
may be ordered in other languages.
The operator is to inform the manufacturer immediately
about all safety related incidents which take place during
operation of the apparatus.

2.6 Safety elements

The apparatus is fitted with a thermal overload protection
for the compressor and the pump.
The minimum quantity of cooling liquid is controlled by a
niveau sensor..

BÜCHI

Recirculating Chiller

B-740

3 Function

The  Büchi  Recirculating  Chiller  B-740  is  a  closed-circuit
cooler  for  use  with  rotary  evaporators.  The  two  models
are distinguished by their outputs.  The 800 watt version
is optimal for cooling one laboratory rotary evaporator, the
1400 watt version is sufficient for cooling two rotary evapo-
rators. The 2500 watt version has enough cooling capacity
to perfectly fit to Rotavapor R-220.

The temperature range extends from -10°C to 20°C, alt-
hough heating is not possible. The B-740 regulates the
temperature to within +/- 1 K exactly. The desired value
is simply entered with two keys (UP and DOWN) and can
be easily read from the LCD display (desired and actual
temperatures).

The environmentally-friendly refrigerant R134a is used as
the refrigerating medium.

3 Function

BÜCHI

Recirculating Chiller

B-740

Check whether the voltage of the socket outlet is the same
as the voltage given on the apparatus plate. Do not turn
the apparatus on before the refrigerant has been added
and the rotary evaporator is connected.

The apparatus must have a minimum distance of 40 cm
between itself and the wall, both in front and behind (suf-
ficient cooling).

• Place the B-740 on a horizontally level, solid base

• Connect out flow and return flow connections of the
B-740 with the cooler of the rotary evaporator. Only
use hoses which can withstand min. -10°C and 1 bar
pressure and secure these with the usual hose clamps.

• Close the drain cock

• Fill the cooling liquid in the filling connections (approx.
2/3 of the inspection glass level) We recommend a
mixture of ethylene glycol 30/70, which does not freeze
until -15°C

• Connect B-740 to electricity supply

4 Putting into operation

Figure 3: Draincock 2500W

Figure 4: Fillingconnection 1 Figure 5: Fillingconnection 2

4 Putting into operation

B-740/25

To avoid the rattling of the compressor heating when the
chiller is started, please consider the following:

• Connect the chiller to the power supply at least 1 hour

before start-up, but do not switch it on, yet.

• Keep the chiller connected to the power supply during

the entire operation.

• After the power supply was interrupted, connect the

chiller to the power supply at least 1 hour before start-
up, but do not switch it on, yet.

BÜCHI

Recirculating Chiller

B-740

5 Operation

Turn on apparatus

Key

Operation

Display

Function

e. g. 25.0
(actual temp.)

• Displays the actual temperature
• Set desired temperature compressor start
• Circulation pump is running

SET

shortly
press

e.g. 10.0

• Display the set temperature

SET +

press

e.g. 10.00

• Increase the desired set temperature in steps of 0.1°C

SET +

∇

press

e.g. 10.0

• Decrease the desired set temperature in steps of 0.1°C

The apparatus is not splash-proof.

5.1 Operatingelements

SET

Indicate set temperature

Increase set temperature

∇

Reduce set temperature

WARNING

indicator in the case of malfunction

COOLING

Cooling indicator

PUMP

Indicator for circulating pump

desired set temperature achieved,
regulation runs

5 Operation

The COOLING and PUMP lamps are always on in normal
operation.

Figure 6: Operating component

BÜCHI

Recirculating Chiller

B-740

6 Maintenance

All  information  which  is  directed  at  maintaining  the  Re-
circulating  Chiller  in  an  operationally  reliable  condition  is
to observed.  This also includes a periodic cleaning and
inspection for possible damage.

6.1 Cleaning

The housing is to be cleaned with a damp cloth without
the use of solvents and to be inspected visually for damage
(operating elements, plug).

Empty contaminated cooling liquid by means of the drain
cock and renew.

6.2 Customer service

Operations on or in the apparatus can only be carried out
by authorized service personnel.  These are persons with
a sound technical training and knowledge of the dangers
which  can  result  from  not  following  safety  precautions.
Büchi  customer  service  centers  have  apparatus-specific
service  manuals  which  are  available  only  to  authorized
personnel.

The addresses of official Büchi customer service centers
are given on the last jacket page of these operating instruc-
tions. Büchi company customer service is available for the
following services: replacement parts service (please refer
to the order number as listed in the operating instructions),
repair service, maintenance service and technical advice.
Please contact the Büchi representative in your country by
telephone, or by fax or telex.

BÜCHI

Recirculating Chiller

B-740

6 Maintenance

6.3 Functional inspection

After every operation, the following parameters are to be
checked:
• Filling level cooling liquid
• Turning on the B-740
• Cooling on / Pump on
• Control set point value

6.4 Malfunctions and their rectification

Table 4: Malfunctions and their rectification

Malfunction

Possible cause

Remedy

Warnung on
Colling off
Pump on

Ambient temperature too high

Soiled liquidator

Change position of the apparatus

Remove front plate; clean lamella with brush or
hoover

Warnung on
Colling off
Pump on

no / too few cooling liquid

Pumpe defekt

Fill up cooling liquid

Please contact customer service

BÜCHI

Recirculating Chiller

B-740

7 Taking out of operation

7.1 Storage/shipping

The cooling liquid is to be drained before storage or ship-
ping. The apparatus is to be stored in the original packaging
in a dry location. Shipping is also to be done in the original
packaging.

7.2 Disposal

In order that the apparatus be disposed of in the most
proenvironmental manner possible, there is in Chapter
8.2, Materials used, a list of the most important parts.
In this way it is ensured that the parts can be separated
and recycled.

For the disposal of electronic components we refer to re-
gional and local disposal laws and regulations.

7 Taking out of operation

BÜCHI

Recirculating Chiller

B-740

B-740/8

B-740/14

B-740/25

Supply voltage

230 V, 50 Hz

230 V, 50/60 Hz

230 V, 50 Hz

Power consumption

max.750 W

max.1200 W

max.1800 W

Display

digital, resolution 0.5 K

Temperature constancy

±1 K

Cooling power at 15°C

800 W

1400 W

2500 W

Pump throughput (max.)

3 l/min

11 l/min

Pumping pressure (max.)

0.6 bar

1 bar

Refrigerant

R134a

Apparatus dimensions
w x h x d/mm

400 x 570 x 450

400 x 670 x 450

550 x 1100 x 450

Weight

Ambient temperature

+15°C...+32°C

Tank volume

5 l

20 l

8 Appendix

8.1 Technical data

8.2 Materials used

Part

Materials

Material code

Housing

Stainless steel

Lamina

Polyester

PES

Circuit board

Glass fiber rein-
forced epoxy
resin

Cable

Polyvinyl chloride PVC

Refrigerant

R134a

Table 6: Materials used

Table 5: Technical data

BÜCHI

Recirculating Chiller

B-740

9 Appendix

8.3 EC conformity declaration

Konformitätserklärung

Declaration of Confirmity

Chiller B-741
Recirculating Chiller B-740
Dehumidifier B-296

- EN 61010-1 /2002-08

- EN 61010-2-010/ A1

- EN 61326 -1:2006

2006/95/EC
2004/108/EC
2006/42/EC

Freital, 06.April 2009

( Hans-Jörg Kupka, Owner)

BÜCHI

Labortechnik AG

CH-9230

Flawil 1 / Switzerland

T +41 71 394 63 63
F +41 71 394 65 65

www.buchi.com

Quality in your hands